Information card for entry 7032040

Structure parameters

• Formula: C181 H206 As4 Cl10 N8 Pd4
• Calculated formula: C181 H206 As4 Cl10 N8 Pd4
• Title of publication: A new library of arsine, stibine-stabilized N-heterocyclic carbene palladium complexes: synthesis, structures and activities in C-C and C-N coupling reactions.
• Authors of publication: Yang, Jin; Li, Pinhua; Zhang, Yicheng; Wang, Lei
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 37
• Pages of publication: 14114 - 14122
• a: 24.87 ± 0.006 Å
• b: 19.199 ± 0.005 Å
• c: 18.773 ± 0.004 Å
• α: 90°
• β: 101.939 ± 0.005°
• γ: 90°
• Cell volume: 8770 ± 4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1354
• Residual factor for significantly intense reflections: 0.0525
• Weighted residual factors for significantly intense reflections: 0.1043
• Weighted residual factors for all reflections included in the refinement: 0.1352
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No