Information card for entry 7032041

Structure parameters

• Formula: C91 H104 Cl6 N4 Pd2 Sb2
• Calculated formula: C91 H104 Cl6 N4 Pd2 Sb2
• Title of publication: A new library of arsine, stibine-stabilized N-heterocyclic carbene palladium complexes: synthesis, structures and activities in C-C and C-N coupling reactions.
• Authors of publication: Yang, Jin; Li, Pinhua; Zhang, Yicheng; Wang, Lei
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 37
• Pages of publication: 14114 - 14122
• a: 31.143 ± 0.006 Å
• b: 13.853 ± 0.003 Å
• c: 23.658 ± 0.005 Å
• α: 90°
• β: 114.411 ± 0.003°
• γ: 90°
• Cell volume: 9294 ± 3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0436
• Residual factor for significantly intense reflections: 0.0308
• Weighted residual factors for significantly intense reflections: 0.0688
• Weighted residual factors for all reflections included in the refinement: 0.0765
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No