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Information card for entry 7032169
Preview
Coordinates | 7032169.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H31 Cl2 F6 Mn N2 O3 P2 |
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Calculated formula | C22 H31 Cl2 F6 Mn N2 O3 P2 |
Title of publication | Aspects of the coordination chemistry of rac-trans-1,2-diphosphinocyclohexane and the preparation of reinforced 9aneP3 and 9anePN2 macrocycles. |
Authors of publication | Edwards, Peter G.; Kariuki, Benson M.; Newman, Paul D.; Tallis, Huw A.; Williams, Craig |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2014 |
Journal volume | 43 |
Journal issue | 41 |
Pages of publication | 15532 - 15545 |
a | 14.229 ± 0.0002 Å |
b | 14.443 ± 0.0003 Å |
c | 16.823 ± 0.0004 Å |
α | 72.145 ± 0.001° |
β | 73.336 ± 0.001° |
γ | 72.418 ± 0.001° |
Cell volume | 3064.39 ± 0.11 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1156 |
Residual factor for significantly intense reflections | 0.0692 |
Weighted residual factors for significantly intense reflections | 0.168 |
Weighted residual factors for all reflections included in the refinement | 0.193 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.03 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7032169.html
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