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Information card for entry 7032170
Preview
Coordinates | 7032170.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C32 H34 F I Mn O4 P3 |
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Calculated formula | C32 H34 F I Mn O4 P3 |
Title of publication | Aspects of the coordination chemistry of rac-trans-1,2-diphosphinocyclohexane and the preparation of reinforced 9aneP3 and 9anePN2 macrocycles. |
Authors of publication | Edwards, Peter G.; Kariuki, Benson M.; Newman, Paul D.; Tallis, Huw A.; Williams, Craig |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2014 |
Journal volume | 43 |
Journal issue | 41 |
Pages of publication | 15532 - 15545 |
a | 35.176 ± 0.005 Å |
b | 10.9232 ± 0.0015 Å |
c | 20.217 ± 0.002 Å |
α | 90° |
β | 113.514 ± 0.009° |
γ | 90° |
Cell volume | 7123 ± 1.6 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 12 |
Hermann-Mauguin space group symbol | C 1 2/m 1 |
Hall space group symbol | -C 2y |
Residual factor for all reflections | 0.116 |
Residual factor for significantly intense reflections | 0.0821 |
Weighted residual factors for significantly intense reflections | 0.1991 |
Weighted residual factors for all reflections included in the refinement | 0.2248 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.085 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7032170.html
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