Information card for entry 7032494

Structure parameters

• Formula: C38 H76 N4 O2 Pb2 S2 Si4
• Calculated formula: C38 H76 N4 O2 Pb2 S2 Si4
• SMILES: C[Si](C)(N([Pb]1[O](C(C)(C)CSc2ccccc2CN(C)C)[Pb](N([Si](C)(C)C)[Si](C)(C)C)[O]1C(C)(C)CSc1ccccc1CN(C)C)[Si](C)(C)C)C
• Title of publication: On the coordination chemistry of organochalcogenolates R(NMe2)^E(-) and R(NMe2)^E^O(-) (E = S, Se) onto lead(ii) and lighter divalent tetrel elements.
• Authors of publication: Pop, Alexandra; Wang, Lingfang; Dorcet, Vincent; Roisnel, Thierry; Carpentier, Jean-François; Silvestru, Anca; Sarazin, Yann
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 43
• Pages of publication: 16459 - 16474
• a: 8.9509 ± 0.0003 Å
• b: 10.6875 ± 0.0004 Å
• c: 13.9731 ± 0.0005 Å
• α: 102.171 ± 0.001°
• β: 103.79 ± 0.002°
• γ: 93.813 ± 0.001°
• Cell volume: 1259.36 ± 0.08 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0206
• Residual factor for significantly intense reflections: 0.0185
• Weighted residual factors for significantly intense reflections: 0.0424
• Weighted residual factors for all reflections included in the refinement: 0.0432
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No