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Information card for entry 7032499
Preview
Coordinates | 7032499.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C105 H58 B4 Cl14 F60 N4 O2 Pb2 Se2 |
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Calculated formula | C98 H44 B4 F60 N4 O2 Pb2 Se2 |
SMILES | [Pb]123[Se](CC(C)(C)[O]2[Pb]24[Se](CC(C)(C)[O]34)c3ccccc3C[N]2(C)C)c2ccccc2C[N]1(C)C.c1(c(c(c(c(c1F)F)F)F)F)[B](c1c(c(c(c(c1F)F)F)F)F)(c1c(c(c(c(c1F)F)F)F)F)[NH2][B](c1c(c(c(c(c1F)F)F)F)F)(c1c(c(c(c(c1F)F)F)F)F)c1c(c(c(c(c1F)F)F)F)F.c1(c(c(c(c(c1F)F)F)F)F)[B](c1c(c(c(c(c1F)F)F)F)F)(c1c(c(c(c(c1F)F)F)F)F)[NH2][B](c1c(c(c(c(c1F)F)F)F)F)(c1c(c(c(c(c1F)F)F)F)F)c1c(c(c(c(c1F)F)F)F)F |
Title of publication | On the coordination chemistry of organochalcogenolates R(NMe2)^E(-) and R(NMe2)^E^O(-) (E = S, Se) onto lead(ii) and lighter divalent tetrel elements. |
Authors of publication | Pop, Alexandra; Wang, Lingfang; Dorcet, Vincent; Roisnel, Thierry; Carpentier, Jean-François; Silvestru, Anca; Sarazin, Yann |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2014 |
Journal volume | 43 |
Journal issue | 43 |
Pages of publication | 16459 - 16474 |
a | 11.9038 ± 0.0006 Å |
b | 14.3044 ± 0.0007 Å |
c | 32.5897 ± 0.0018 Å |
α | 90° |
β | 90.138 ± 0.002° |
γ | 90° |
Cell volume | 5549.3 ± 0.5 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 9 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0673 |
Residual factor for significantly intense reflections | 0.0604 |
Weighted residual factors for significantly intense reflections | 0.1561 |
Weighted residual factors for all reflections included in the refinement | 0.1612 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.021 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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