Information card for entry 7032846

Structure parameters

• Formula: C28 H32 N14 O11 Pb2
• Calculated formula: C22 H16 N12 O8 Pb2
• Title of publication: Synthesis, structure and catalytic application of lead(II) complexes in cyanosilylation reactions.
• Authors of publication: Karmakar, Anirban; Hazra, Susanta; Guedes da Silva, M Fátima C; Pombeiro, Armando J. L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 1
• Pages of publication: 268 - 280
• a: 7.8443 ± 0.0004 Å
• b: 22.1845 ± 0.0013 Å
• c: 21.7657 ± 0.0013 Å
• α: 90°
• β: 90.842 ± 0.002°
• γ: 90°
• Cell volume: 3787.3 ± 0.4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0862
• Residual factor for significantly intense reflections: 0.0526
• Weighted residual factors for significantly intense reflections: 0.1172
• Weighted residual factors for all reflections included in the refinement: 0.1269
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No