Information card for entry 7032847

Structure parameters

• Formula: C20 H16 N12 O8 Pb2
• Calculated formula: C20 H16 N12 O8 Pb2
• SMILES: c1([n]2ccnc1N)C(=O)[O]1[Pb]23([n]4c(c(ncc4)N)C(=O)O3)[O]2C(=O)c3c(ncc[n]3[Pb]312[n]1c(C(=O)O3)c(ncc1)N)N
• Title of publication: Synthesis, structure and catalytic application of lead(II) complexes in cyanosilylation reactions.
• Authors of publication: Karmakar, Anirban; Hazra, Susanta; Guedes da Silva, M Fátima C; Pombeiro, Armando J. L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 1
• Pages of publication: 268 - 280
• a: 7.752 ± 0.0003 Å
• b: 7.8081 ± 0.0003 Å
• c: 11.2756 ± 0.0005 Å
• α: 85.184 ± 0.002°
• β: 86.853 ± 0.002°
• γ: 67.114 ± 0.001°
• Cell volume: 626.36 ± 0.04 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.022
• Residual factor for significantly intense reflections: 0.0214
• Weighted residual factors for significantly intense reflections: 0.054
• Weighted residual factors for all reflections included in the refinement: 0.0544
• Goodness-of-fit parameter for all reflections included in the refinement: 1.166
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No