Information card for entry 7032848

Structure parameters

• Formula: C14 H16 N8 O10 Pb2
• Calculated formula: C14 H16 N8 O10 Pb2
• SMILES: c12c(ncc[n]1[Pb]1(OC=O)[O](C2=O)[Pb]2([n]3c(C(=O)[O]12)c(ncc3)N)OC=O)N.C(=O)N.C(=O)N
• Title of publication: Synthesis, structure and catalytic application of lead(II) complexes in cyanosilylation reactions.
• Authors of publication: Karmakar, Anirban; Hazra, Susanta; Guedes da Silva, M Fátima C; Pombeiro, Armando J. L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 1
• Pages of publication: 268 - 280
• a: 7.6846 ± 0.0004 Å
• b: 8.025 ± 0.0004 Å
• c: 10.1201 ± 0.0005 Å
• α: 102.495 ± 0.002°
• β: 99.181 ± 0.002°
• γ: 112.272 ± 0.003°
• Cell volume: 543.33 ± 0.05 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0192
• Residual factor for significantly intense reflections: 0.0187
• Weighted residual factors for significantly intense reflections: 0.0458
• Weighted residual factors for all reflections included in the refinement: 0.0462
• Goodness-of-fit parameter for all reflections included in the refinement: 1.19
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No