Information card for entry 7033090

Structure parameters

• Formula: C31 H53 K2 N O12 S4
• Calculated formula: C31 H53 K2 N O12 S4
• Title of publication: CS2 activation at uranium(iii) siloxide ate complexes: the effect of a Lewis acidic site.
• Authors of publication: Camp, Clément; Cooper, Oliver; Andrez, Julie; Pécaut, Jacques; Mazzanti, Marinella
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 6
• Pages of publication: 2650 - 2656
• a: 23.321 ± 0.003 Å
• b: 10.1497 ± 0.0005 Å
• c: 21.907 ± 0.003 Å
• α: 90°
• β: 127.579 ± 0.019°
• γ: 90°
• Cell volume: 4109.5 ± 1.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1109
• Residual factor for significantly intense reflections: 0.0611
• Weighted residual factors for significantly intense reflections: 0.1339
• Weighted residual factors for all reflections included in the refinement: 0.1557
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No