Information card for entry 7033091

Structure parameters

• Formula: C101 H188 K2 O28 S3 Si4 U
• Calculated formula: C101 H188 K2 O28 S3 Si4 U
• Title of publication: CS2 activation at uranium(iii) siloxide ate complexes: the effect of a Lewis acidic site.
• Authors of publication: Camp, Clément; Cooper, Oliver; Andrez, Julie; Pécaut, Jacques; Mazzanti, Marinella
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 6
• Pages of publication: 2650 - 2656
• a: 14.8483 ± 0.0006 Å
• b: 17.9359 ± 0.0008 Å
• c: 25.5598 ± 0.0012 Å
• α: 81.725 ± 0.004°
• β: 85.15 ± 0.003°
• γ: 76.692 ± 0.004°
• Cell volume: 6545.9 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1344
• Residual factor for significantly intense reflections: 0.0919
• Weighted residual factors for significantly intense reflections: 0.2028
• Weighted residual factors for all reflections included in the refinement: 0.2231
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No