Information card for entry 7033476

Structure parameters

• Formula: C68 H138 Co9 N3 O36
• Calculated formula: C68 H138 Co9 N3 O36
• Title of publication: Switching nuclearity and Co(ii) content through stoichiometry adjustment: {Co(II)6Co(III)3} and {Co(II)Co4(III)} mixed valent complexes and a study of their magnetic properties.
• Authors of publication: Funes, Alejandro V.; Carrella, Luca; Sorace, Lorenzo; Rentschler, Eva; Alborés, Pablo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 5
• Pages of publication: 2390 - 2400
• a: 14.7903 ± 0.0015 Å
• b: 15.2087 ± 0.0012 Å
• c: 25.894 ± 0.002 Å
• α: 91.97 ± 0.006°
• β: 104.308 ± 0.008°
• γ: 118.052 ± 0.009°
• Cell volume: 4903.1 ± 0.9 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1849
• Residual factor for significantly intense reflections: 0.101
• Weighted residual factors for significantly intense reflections: 0.2287
• Weighted residual factors for all reflections included in the refinement: 0.3027
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No