Information card for entry 7033477

Structure parameters

• Formula: C46 H90.8 Co5 N5 O26
• Calculated formula: C46 H90.8 Co5 N5 O26
• Title of publication: Switching nuclearity and Co(ii) content through stoichiometry adjustment: {Co(II)6Co(III)3} and {Co(II)Co4(III)} mixed valent complexes and a study of their magnetic properties.
• Authors of publication: Funes, Alejandro V.; Carrella, Luca; Sorace, Lorenzo; Rentschler, Eva; Alborés, Pablo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 5
• Pages of publication: 2390 - 2400
• a: 20.3316 ± 0.0007 Å
• b: 10.9609 ± 0.0005 Å
• c: 28.8394 ± 0.0012 Å
• α: 90°
• β: 108.706 ± 0.004°
• γ: 90°
• Cell volume: 6087.4 ± 0.5 ų
• Cell temperature: 151 ± 1 K
• Ambient diffraction temperature: 151 ± 1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1067
• Residual factor for significantly intense reflections: 0.0624
• Weighted residual factors for significantly intense reflections: 0.1179
• Weighted residual factors for all reflections included in the refinement: 0.1387
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No