Information card for entry 7033524

Structure parameters

• Formula: C48 H40 N2 P4 Te5
• Calculated formula: C48 H40 N2 P4 Te5
• Title of publication: Sodium and rhodium complexes of a spirocyclic Te5 dianion supported by P2N2 rings.
• Authors of publication: Nordheider, Andreas; Athukorala Arachchige, Kasun S.; Slawin, Alexandra M. Z.; Woollins, J. Derek; Chivers, Tristram
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 19
• Pages of publication: 8781 - 8783
• a: 11.021 ± 0.002 Å
• b: 14.951 ± 0.003 Å
• c: 15.893 ± 0.003 Å
• α: 90°
• β: 113.47 ± 0.03°
• γ: 90°
• Cell volume: 2402.1 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0583
• Residual factor for significantly intense reflections: 0.0342
• Weighted residual factors for significantly intense reflections: 0.0714
• Weighted residual factors for all reflections included in the refinement: 0.0822
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No