Information card for entry 7034030

Structure parameters

• Formula: C30 H40 Ag3 Cl3 N8 O12
• Calculated formula: C30 H40 Ag3 Cl3 N8 O12
• Title of publication: Macrocyclic dinuclear, helical, layered and 3-D Ag(i) complexes constructed from AgX (X = NO3(-) and ClO4(-)) and flexible bis(pyridyl) ligands with a chelating spacer: syntheses, structures and photoluminescence properties.
• Authors of publication: Huang, Jing; Deng, Zhao-Peng; Xiao, Ying-Hui; Huo, Li-Hua; Zhao, Shu-Nan; Ge, Fa-Yuan; Gao, Shan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 12
• Pages of publication: 5837 - 5847
• a: 14.966 ± 0.002 Å
• b: 13.205 ± 0.002 Å
• c: 23.389 ± 0.003 Å
• α: 90°
• β: 118.964 ± 0.009°
• γ: 90°
• Cell volume: 4044.1 ± 1 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1058
• Residual factor for significantly intense reflections: 0.0609
• Weighted residual factors for significantly intense reflections: 0.134
• Weighted residual factors for all reflections included in the refinement: 0.1558
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No