Information card for entry 7034195

Structure parameters

• Formula: C63 H65 N3 O P2
• Calculated formula: C63 H65 N3 O P2
• Title of publication: A stable phosphanyl phosphaketene and its reactivity.
• Authors of publication: Li, Zhongshu; Chen, Xiaodan; Bergeler, Maike; Reiher, Markus; Su, Cheng-Yong; Grützmacher, Hansjörg
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 14
• Pages of publication: 6431 - 6438
• a: 17.7901 ± 0.0014 Å
• b: 18.7231 ± 0.0016 Å
• c: 19.1169 ± 0.0016 Å
• α: 73.099 ± 0.003°
• β: 63.618 ± 0.003°
• γ: 71.027 ± 0.003°
• Cell volume: 5313.5 ± 0.8 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100.7 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.085
• Residual factor for significantly intense reflections: 0.064
• Weighted residual factors for significantly intense reflections: 0.168
• Weighted residual factors for all reflections included in the refinement: 0.1827
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No