Information card for entry 7034194

Structure parameters

• Formula: C33 H46 N2 O P2
• Calculated formula: C33 H46 N2 O P2
• Title of publication: A stable phosphanyl phosphaketene and its reactivity.
• Authors of publication: Li, Zhongshu; Chen, Xiaodan; Bergeler, Maike; Reiher, Markus; Su, Cheng-Yong; Grützmacher, Hansjörg
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 14
• Pages of publication: 6431 - 6438
• a: 11.3904 ± 0.0005 Å
• b: 20.3999 ± 0.0009 Å
• c: 13.5469 ± 0.0006 Å
• α: 90°
• β: 93.823 ± 0.003°
• γ: 90°
• Cell volume: 3140.8 ± 0.2 ų
• Cell temperature: 101 ± 2 K
• Ambient diffraction temperature: 100.8 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1
• Residual factor for significantly intense reflections: 0.0774
• Weighted residual factors for significantly intense reflections: 0.1799
• Weighted residual factors for all reflections included in the refinement: 0.1971
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No