Information card for entry 7034222

Structure parameters

• Formula: C21 H50 Cl7 Nb O7 Sn2
• Calculated formula: C21 H50 Cl7 Nb O7 Sn2
• Title of publication: A convenient and quantitative route to Sn(iv)-M [M = Ti(iv), Nb(v), Ta(v)] heterobimetallic precursors for dense mixed-metal oxide ceramics.
• Authors of publication: Mishra, Shashank; Jeanneau, Erwann; Mangematin, Stéphane; Chermette, Henry; Poor Kalhor, Mahboubeh; Bonnefont, Guillaume; Fantozzi, Gilbert; Le Floch, Sylvie; Pailhes, Stéphane; Daniele, Stéphane
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 15
• Pages of publication: 6848 - 6862
• a: 9.2836 ± 0.0006 Å
• b: 10.752 ± 0.0007 Å
• c: 20.6254 ± 0.001 Å
• α: 83.935 ± 0.005°
• β: 79.557 ± 0.006°
• γ: 68.034 ± 0.006°
• Cell volume: 1876.1 ± 0.2 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0513
• Residual factor for significantly intense reflections: 0.0395
• Weighted residual factors for all reflections: 0.1109
• Weighted residual factors for significantly intense reflections: 0.1053
• Weighted residual factors for all reflections included in the refinement: 0.1109
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9527
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No