Information card for entry 7034303

Structure parameters

• Formula: C38 H64 Cl3 Li N2 O2 Si Zr
• Calculated formula: C38 H64 Cl3 Li N2 O2 Si Zr
• Title of publication: Synthesis, characterisation, and dehydrocoupling ability of zirconium complexes bearing hindered bis(amido)silyl ligands.
• Authors of publication: Lummis, Paul A.; McDonald, Robert; Ferguson, Michael J.; Rivard, Eric
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 15
• Pages of publication: 7009 - 7020
• a: 10.2481 ± 0.0004 Å
• b: 27.2915 ± 0.0011 Å
• c: 15.7628 ± 0.0006 Å
• α: 90°
• β: 101.817 ± 0.0004°
• γ: 90°
• Cell volume: 4315.2 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0423
• Residual factor for significantly intense reflections: 0.0379
• Weighted residual factors for significantly intense reflections: 0.0961
• Weighted residual factors for all reflections included in the refinement: 0.0989
• Goodness-of-fit parameter for all reflections included in the refinement: 1.112
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No