Information card for entry 7034644

Structure parameters

• Formula: C33 H60 N4 O0.5 Si4 Zn
• Calculated formula: C32.998 H60 N4 O0.5 Si3.9975 Zn
• Title of publication: Two alternative approaches to access mixed hydride-amido zinc complexes: synthetic, structural and solution implications.
• Authors of publication: Roberts, Andrew J.; Clegg, William; Kennedy, Alan R.; Probert, Michael R.; Robertson, Stuart D.; Hevia, Eva
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 17
• Pages of publication: 8169 - 8177
• a: 21.938 ± 0.002 Å
• b: 18.8738 ± 0.0014 Å
• c: 21.985 ± 0.004 Å
• α: 90°
• β: 119.304 ± 0.015°
• γ: 90°
• Cell volume: 7938 ± 2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1557
• Residual factor for significantly intense reflections: 0.07
• Weighted residual factors for significantly intense reflections: 0.1001
• Weighted residual factors for all reflections included in the refinement: 0.125
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No