Information card for entry 7035150

Structure parameters

• Formula: C37 H54 Fe Ge N4 O4 Si2
• Calculated formula: C37 H54 Fe Ge N4 O4 Si2
• SMILES: [Ge]([Fe](C#[O])(C#[O])(C#[O])C#[O])(N=C1N(C=CN1c1c(cccc1C(C)C)C(C)C)c1c(cccc1C(C)C)C(C)C)N([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Isolation of a germanium(ii) cation and a germylene iron carbonyl complex utilizing an imidazolin-2-iminato ligand.
• Authors of publication: Ochiai, Tatsumi; Franz, Daniel; Wu, Xiao-Nan; Inoue, Shigeyoshi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 24
• Pages of publication: 10952 - 10956
• a: 20.6549 ± 0.0002 Å
• b: 20.4224 ± 0.0001 Å
• c: 22.6744 ± 0.0002 Å
• α: 90°
• β: 116.955 ± 0.001°
• γ: 90°
• Cell volume: 8525.51 ± 0.14 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0545
• Residual factor for significantly intense reflections: 0.0376
• Weighted residual factors for significantly intense reflections: 0.0896
• Weighted residual factors for all reflections included in the refinement: 0.0987
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No