Information card for entry 7035151

Structure parameters

• Formula: C51 H54 B F15 Ge N4 Si2
• Calculated formula: C51 H54 B F15 Ge N4 Si2
• SMILES: [Ge]1N([Si](C)(C)C)[Si]([N]1=C1N(C=CN1c1c(cccc1C(C)C)C(C)C)c1c(cccc1C(C)C)C(C)C)(C)C.Fc1c([B](c2c(F)c(F)c(F)c(F)c2F)(c2c(F)c(F)c(F)c(F)c2F)C)c(F)c(F)c(F)c1F
• Title of publication: Isolation of a germanium(ii) cation and a germylene iron carbonyl complex utilizing an imidazolin-2-iminato ligand.
• Authors of publication: Ochiai, Tatsumi; Franz, Daniel; Wu, Xiao-Nan; Inoue, Shigeyoshi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 24
• Pages of publication: 10952 - 10956
• a: 11.907 ± 0.0004 Å
• b: 14.4773 ± 0.0004 Å
• c: 16.6752 ± 0.0005 Å
• α: 76.511 ± 0.002°
• β: 72.772 ± 0.003°
• γ: 88.005 ± 0.002°
• Cell volume: 2667.97 ± 0.15 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0359
• Residual factor for significantly intense reflections: 0.0326
• Weighted residual factors for significantly intense reflections: 0.1191
• Weighted residual factors for all reflections included in the refinement: 0.1284
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No