Information card for entry 7035228

Structure parameters

• Formula: C10 H20 F6 O2 P2 Pb Si
• Calculated formula: C10 H20 F6 O2 P2 Pb Si
• Title of publication: Lead(ii) nitrate and hexafluorosilicate complexes with neutral diphosphine coordination.
• Authors of publication: Burt, Jennifer; Grantham, William; Levason, William; Reid, Gillian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 25
• Pages of publication: 11533 - 11541
• a: 6.6164 ± 0.0017 Å
• b: 10.637 ± 0.003 Å
• c: 12.354 ± 0.003 Å
• α: 93.58 ± 0.006°
• β: 93.952 ± 0.003°
• γ: 100.854 ± 0.006°
• Cell volume: 849.3 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0276
• Residual factor for significantly intense reflections: 0.0261
• Weighted residual factors for significantly intense reflections: 0.0643
• Weighted residual factors for all reflections included in the refinement: 0.0646
• Goodness-of-fit parameter for all reflections included in the refinement: 0.996
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No