Information card for entry 7035229

Structure parameters

• Formula: C19 H37 F6 N3 O3 P2 Pb Si
• Calculated formula: C19 H37 F6 N3 O3 P2 Pb Si
• SMILES: [Pb]1([P](c2ccccc2[P]1(C)C)(C)C)([F][Si](F)(F)(F)(F)F)[O]=CN(C)C.O=CN(C)C.O=CN(C)C
• Title of publication: Lead(ii) nitrate and hexafluorosilicate complexes with neutral diphosphine coordination.
• Authors of publication: Burt, Jennifer; Grantham, William; Levason, William; Reid, Gillian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 25
• Pages of publication: 11533 - 11541
• a: 8.404 ± 0.002 Å
• b: 10.352 ± 0.003 Å
• c: 15.994 ± 0.005 Å
• α: 87.522 ± 0.007°
• β: 89.782 ± 0.006°
• γ: 86.063 ± 0.007°
• Cell volume: 1386.9 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0477
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for significantly intense reflections: 0.0869
• Weighted residual factors for all reflections included in the refinement: 0.088
• Goodness-of-fit parameter for all reflections included in the refinement: 0.887
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No