Information card for entry 7035231

Structure parameters

• Formula: C12.5 H33.5 B2 F8 N0.5 O3 P4 Pb
• Calculated formula: C12.5 H32 B2 F8 N0.5 O3 P4 Pb
• Title of publication: Lead(ii) nitrate and hexafluorosilicate complexes with neutral diphosphine coordination.
• Authors of publication: Burt, Jennifer; Grantham, William; Levason, William; Reid, Gillian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 25
• Pages of publication: 11533 - 11541
• a: 16.938 ± 0.006 Å
• b: 24.212 ± 0.009 Å
• c: 25.686 ± 0.01 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10534 ± 7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 70
• Hermann-Mauguin space group symbol: F d d d
• Hall space group symbol: -F 2uv 2vw
• Residual factor for all reflections: 0.0613
• Residual factor for significantly intense reflections: 0.0527
• Weighted residual factors for significantly intense reflections: 0.1033
• Weighted residual factors for all reflections included in the refinement: 0.1075
• Goodness-of-fit parameter for all reflections included in the refinement: 1.146
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No