Information card for entry 7035230

Structure parameters

• Formula: C20 H48 N2 O10 P4 Pb
• Calculated formula: C20 H48 N2 O10 P4 Pb
• Title of publication: Lead(ii) nitrate and hexafluorosilicate complexes with neutral diphosphine coordination.
• Authors of publication: Burt, Jennifer; Grantham, William; Levason, William; Reid, Gillian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 25
• Pages of publication: 11533 - 11541
• a: 15.1483 ± 0.0005 Å
• b: 13.89 ± 0.0004 Å
• c: 16.2854 ± 0.0005 Å
• α: 90°
• β: 112.383 ± 0.003°
• γ: 90°
• Cell volume: 3168.45 ± 0.18 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0446
• Residual factor for significantly intense reflections: 0.031
• Weighted residual factors for significantly intense reflections: 0.0674
• Weighted residual factors for all reflections included in the refinement: 0.073
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No