Information card for entry 7035242

Structure parameters

• Common name: [Ni(phen)2]2Sn2S6*4,4'-bipy*1/2H2O
• Chemical name: {[Ni(C12H8N2)2]2Sn2S6*C10H8N2*1/2H2O
• Formula: C58 H42 N10 Ni2 O S6 Sn2
• Calculated formula: C58 H42 N10 Ni2 O S6 Sn2
• Title of publication: Utilization of mixtures of aromatic N-donor ligands of different coordination ability for the solvothermal synthesis of thiostannate containing molecules.
• Authors of publication: Hilbert, J.; Näther, C; Bensch, W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 25
• Pages of publication: 11542 - 11550
• a: 18.3431 ± 0.0006 Å
• b: 19.4475 ± 0.0006 Å
• c: 15.0835 ± 0.0005 Å
• α: 90°
• β: 95.556 ± 0.002°
• γ: 90°
• Cell volume: 5355.4 ± 0.3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0641
• Residual factor for significantly intense reflections: 0.0466
• Weighted residual factors for significantly intense reflections: 0.1038
• Weighted residual factors for all reflections included in the refinement: 0.1113
• Goodness-of-fit parameter for all reflections included in the refinement: 1.084
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No