Information card for entry 7035326

Structure parameters

• Formula: C49 H71 F9 N8 O9 Sb2
• Calculated formula: C49 H71 F9 N8 O9 Sb2
• SMILES: c12c(cccc1C[N]1(CCN(CC1)C)[Sb]132[OH][Sb]23(c3c(cccc3CN3CC[NH+](CC3)C)C[N]32CCN(CC3)C)O1)CN1CC[NH+](CC1)C.C(C(=O)[O-])(F)(F)F.C(C(=O)[O-])(F)(F)F.C(C(=O)[O-])(F)(F)F.O.c1(ccccc1)C
• Title of publication: A general route to monoorganopnicogen(iii) (M = Sb, Bi) compounds with a pincer (N,C,N) group and oxo ligands.
• Authors of publication: Strîmb, Gabriela; Pöllnitz, Alpár; Raţ, Ciprian I; Silvestru, Cristian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 21
• Pages of publication: 9927 - 9942
• a: 11.046 ± 0.0011 Å
• b: 28.78 ± 0.003 Å
• c: 18.4055 ± 0.0018 Å
• α: 90°
• β: 95.829 ± 0.002°
• γ: 90°
• Cell volume: 5820.9 ± 1 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0888
• Residual factor for significantly intense reflections: 0.0568
• Weighted residual factors for significantly intense reflections: 0.1198
• Weighted residual factors for all reflections included in the refinement: 0.1336
• Goodness-of-fit parameter for all reflections included in the refinement: 0.994
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No