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Information card for entry 7035586
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Coordinates | 7035586.cif |
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Original paper (by DOI) | HTML |
Chemical name | 1,3-bis(2,6-diisopropylphenyl)-2-phosphanylideneimidazolidine |
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Formula | C27 H39 N2 P |
Calculated formula | C27 H39 N2 P |
Title of publication | Carbene insertion into a P-H bond: parent phosphinidene-carbene adducts from PH3 and bis(phosphinidene)mercury complexes. |
Authors of publication | Bispinghoff, Mark; Tondreau, Aaron M.; Grützmacher, Hansjörg; Faradji, Charly A.; Pringle, Paul G. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2016 |
Journal volume | 45 |
Journal issue | 14 |
Pages of publication | 5999 - 6003 |
a | 11.8631 ± 0.0006 Å |
b | 20.2676 ± 0.0009 Å |
c | 10.9214 ± 0.0005 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2625.9 ± 0.2 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 K |
Number of distinct elements | 4 |
Space group number | 62 |
Hermann-Mauguin space group symbol | P n m a |
Hall space group symbol | -P 2ac 2n |
Residual factor for all reflections | 0.0645 |
Residual factor for significantly intense reflections | 0.0476 |
Weighted residual factors for significantly intense reflections | 0.1236 |
Weighted residual factors for all reflections included in the refinement | 0.1364 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.021 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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