Information card for entry 7035701

Structure parameters

• Formula: C38 H47 F24 N9 P4
• Calculated formula: C38 H47 F24 N9 P4
• Title of publication: Synthesis of a flexible macrocyclic tetraimidazolium salt-precursor for a tetracarbene ligand with metal dependent coordination modes.
• Authors of publication: Schulte To Brinke, Christian; Ekkehardt Hahn, F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 32
• Pages of publication: 14315 - 14322
• a: 14.3308 ± 0.0008 Å
• b: 13.4896 ± 0.0007 Å
• c: 25.4184 ± 0.0014 Å
• α: 90°
• β: 100.399 ± 0.004°
• γ: 90°
• Cell volume: 4833.1 ± 0.5 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.044
• Residual factor for significantly intense reflections: 0.0399
• Weighted residual factors for significantly intense reflections: 0.1109
• Weighted residual factors for all reflections included in the refinement: 0.1138
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No