Information card for entry 7035928

Structure parameters

• Formula: C47 H42 Cl2 N P Si
• Calculated formula: C47 H42 Cl2 N P Si
• Title of publication: Extremely bulky secondary phosphinoamines as substituents for sterically hindered aminosilanes.
• Authors of publication: Böttcher, Tobias; Jones, Cameron
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 33
• Pages of publication: 14842 - 14853
• a: 9.9729 ± 0.0004 Å
• b: 13.3211 ± 0.0006 Å
• c: 29.4129 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3907.5 ± 0.3 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.064
• Residual factor for significantly intense reflections: 0.052
• Weighted residual factors for significantly intense reflections: 0.1201
• Weighted residual factors for all reflections included in the refinement: 0.1279
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No