Information card for entry 7036096

Structure parameters

• Formula: C17 H43 Mg N O2 Si2
• Calculated formula: C17 H43 Mg N O2 Si2
• SMILES: [Si](N([Si](C)(C)C(C)(C)C)[Mg]1([O](C)CC[O]1C)C)(C)(C)C(C)(C)C
• Title of publication: Salt metathesis versus protonolysis routes for the synthesis of silylamide Hauser base (R2NMgX; X = halogen) and amido-Grignard (R2NMgR) complexes.
• Authors of publication: Goodwin, Conrad A. P.; Smith, Alex; Ortu, Fabrizio; Vitorica-Yrezabal, Iñigo J; Mills, David P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 14
• Pages of publication: 6004 - 6014
• a: 7.7728 ± 0.0004 Å
• b: 9.8848 ± 0.0004 Å
• c: 16.9636 ± 0.001 Å
• α: 87.573 ± 0.004°
• β: 79.144 ± 0.005°
• γ: 70.342 ± 0.004°
• Cell volume: 1205.12 ± 0.11 ų
• Cell temperature: 150.02 ± 0.13 K
• Ambient diffraction temperature: 150.02 ± 0.13 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0531
• Residual factor for significantly intense reflections: 0.0422
• Weighted residual factors for significantly intense reflections: 0.0953
• Weighted residual factors for all reflections included in the refinement: 0.1019
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No