Crystallography Open Database

Information card for entry 7036327

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Coordinates	7036327.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H43 N P2
Calculated formula	C24 H43 N P2
Title of publication	Synthetic strategies to bicyclic tetraphosphanes using P1, P2 and P4 building blocks.
Authors of publication	Bresien, Jonas; Faust, Kirill; Hering-Junghans, Christian; Rothe, Julia; Schulz, Axel; Villinger, Alexander
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	5
Pages of publication	1998 - 2007
a	10.0058 ± 0.0005 Å
b	26.4841 ± 0.0011 Å
c	9.9173 ± 0.0005 Å
α	90°
β	101.035 ± 0.002°
γ	90°
Cell volume	2579.4 ± 0.2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0688
Residual factor for significantly intense reflections	0.05
Weighted residual factors for significantly intense reflections	0.1263
Weighted residual factors for all reflections included in the refinement	0.1407
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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