Crystallography Open Database

Information card for entry 7036328

Preview

Coordinates	7036328.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H47 P Si2
Calculated formula	C24 H47 P Si2
Title of publication	Synthetic strategies to bicyclic tetraphosphanes using P1, P2 and P4 building blocks.
Authors of publication	Bresien, Jonas; Faust, Kirill; Hering-Junghans, Christian; Rothe, Julia; Schulz, Axel; Villinger, Alexander
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	5
Pages of publication	1998 - 2007
a	9.3749 ± 0.0006 Å
b	16.9528 ± 0.0011 Å
c	17.6869 ± 0.001 Å
α	90°
β	101.224 ± 0.003°
γ	90°
Cell volume	2757.2 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0974
Residual factor for significantly intense reflections	0.0475
Weighted residual factors for significantly intense reflections	0.0979
Weighted residual factors for all reflections included in the refinement	0.1154
Goodness-of-fit parameter for all reflections included in the refinement	1.002
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7036328.html