Information card for entry 7036527

Structure parameters

• Formula: C23 H50 Al2 Ho N Si
• Calculated formula: C23 H50 Al2 Ho N Si
• SMILES: [CH3]1[Al](C)(C)[CH3][Ho]21([CH3][Al]([CH3]2)(C)C)N([Si](C)(C)C)c1c(cccc1C(C)C)C(C)C
• Title of publication: Rare-earth metal methylidene complexes with Ln3(μ3-CH2)(μ3-Me)(μ2-Me)3 core structure.
• Authors of publication: Schädle, Dorothea; Meermann-Zimmermann, Melanie; Maichle-Mössmer, Cäcilia; Schädle, Christoph; Törnroos, Karl W; Anwander, Reiner
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 41
• Pages of publication: 18101 - 18110
• a: 12.201 ± 0.003 Å
• b: 17.328 ± 0.008 Å
• c: 28.104 ± 0.008 Å
• α: 90°
• β: 91.7 ± 0.02°
• γ: 90°
• Cell volume: 5939 ± 4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0647
• Residual factor for significantly intense reflections: 0.0433
• Weighted residual factors for significantly intense reflections: 0.069
• Weighted residual factors for all reflections included in the refinement: 0.0738
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No