Information card for entry 7036528

Structure parameters

• Formula: C23 H50 Al2 La N Si
• Calculated formula: C23 H50 Al2 La N Si
• SMILES: [La]12(N([Si](C)(C)C)c3c(cccc3C(C)C)C(C)C)([CH3][Al]([CH3]1)(C)C)[CH3][Al]([CH3]2)(C)C
• Title of publication: Rare-earth metal methylidene complexes with Ln3(μ3-CH2)(μ3-Me)(μ2-Me)3 core structure.
• Authors of publication: Schädle, Dorothea; Meermann-Zimmermann, Melanie; Maichle-Mössmer, Cäcilia; Schädle, Christoph; Törnroos, Karl W; Anwander, Reiner
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 41
• Pages of publication: 18101 - 18110
• a: 9.3816 ± 0.0009 Å
• b: 12.6128 ± 0.0008 Å
• c: 12.757 ± 0.0012 Å
• α: 90°
• β: 94.34 ± 0.008°
• γ: 90°
• Cell volume: 1505.2 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0302
• Residual factor for significantly intense reflections: 0.0278
• Weighted residual factors for significantly intense reflections: 0.0644
• Weighted residual factors for all reflections included in the refinement: 0.0653
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No