Information card for entry 7036778

Structure parameters

• Formula: C43 H53 N2 Nb O2 P3
• Calculated formula: C43 H53 N2 Nb O2 P3
• Title of publication: Assembly and stabilization of {E(cyclo-P3)2} (E = Sn, Pb) as a bridging ligand spanning two triaryloxyniobium units.
• Authors of publication: Velian, Alexandra; Cossairt, Brandi M.; Cummins, Christopher C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 5
• Pages of publication: 1891 - 1895
• a: 14.0102 ± 0.001 Å
• b: 16.5289 ± 0.0012 Å
• c: 18.0957 ± 0.001 Å
• α: 90°
• β: 92.662 ± 0.004°
• γ: 90°
• Cell volume: 4186 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0554
• Residual factor for significantly intense reflections: 0.0388
• Weighted residual factors for significantly intense reflections: 0.0923
• Weighted residual factors for all reflections included in the refinement: 0.1013
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No