Information card for entry 7036779

Structure parameters

• Formula: C78.24 H108.49 Nb2 O6 P6 Sn
• Calculated formula: C78.243 H108.486 Nb2 O6 P6 Sn
• Title of publication: Assembly and stabilization of {E(cyclo-P3)2} (E = Sn, Pb) as a bridging ligand spanning two triaryloxyniobium units.
• Authors of publication: Velian, Alexandra; Cossairt, Brandi M.; Cummins, Christopher C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 5
• Pages of publication: 1891 - 1895
• a: 19.234 ± 0.002 Å
• b: 20.735 ± 0.002 Å
• c: 20.601 ± 0.002 Å
• α: 90°
• β: 92.989 ± 0.002°
• γ: 90°
• Cell volume: 8204.9 ± 1.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0656
• Residual factor for significantly intense reflections: 0.0364
• Weighted residual factors for significantly intense reflections: 0.0692
• Weighted residual factors for all reflections included in the refinement: 0.0796
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No