Information card for entry 7037036

Structure parameters

• Formula: C33 H55 Cl0.48 I0.52 N2 P2 W
• Calculated formula: C33 H55 Cl0.483 I0.517 N2 P2 W
• Title of publication: An investigation on the chemistry of the R2P[double bond, length as m-dash]P ligand: reactions of a phosphanylphosphinidene complex of tungsten(vi) with electrophilic reagents.
• Authors of publication: Grubba, Rafał; Ordyszewska, Anna; Ponikiewski, Łukasz; Gudat, Dietrich; Pikies, Jerzy
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 5
• Pages of publication: 2172 - 2179
• a: 10.0532 ± 0.0005 Å
• b: 11.0185 ± 0.0006 Å
• c: 18.3344 ± 0.0007 Å
• α: 75.349 ± 0.003°
• β: 82.138 ± 0.003°
• γ: 67.418 ± 0.003°
• Cell volume: 1812.45 ± 0.16 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0406
• Residual factor for significantly intense reflections: 0.03
• Weighted residual factors for significantly intense reflections: 0.0583
• Weighted residual factors for all reflections included in the refinement: 0.06
• Goodness-of-fit parameter for all reflections included in the refinement: 0.905
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No