Information card for entry 7037037

Structure parameters

• Formula: C110.15 H161.65 P2 Sn2
• Calculated formula: C110.14 H161.66 P2 Sn2
• Title of publication: Reaction of an allylstannylene with adamantyl phosphaalkyne.
• Authors of publication: Krebs, K. M.; Jamin, J.; Wesemann, L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 14
• Pages of publication: 5933 - 5936
• a: 14.9605 ± 0.0003 Å
• b: 17.8145 ± 0.0004 Å
• c: 19.5352 ± 0.0004 Å
• α: 79.946 ± 0.001°
• β: 82.256 ± 0.001°
• γ: 83.423 ± 0.001°
• Cell volume: 5057.55 ± 0.19 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.093
• Residual factor for significantly intense reflections: 0.0535
• Weighted residual factors for significantly intense reflections: 0.1275
• Weighted residual factors for all reflections included in the refinement: 0.1455
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No