Information card for entry 7037444

Structure parameters

• Formula: C38 H32 Cl O2 P Pd
• Calculated formula: C38 H32 Cl O2 P Pd
• Title of publication: The design of second generation MOP-phosphonites: efficient chiral hydrosilylation of functionalised styrenes.
• Authors of publication: Fleming, James T.; Ficks, Arne; Waddell, Paul G.; Harrington, Ross W.; Higham, Lee J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 5
• Pages of publication: 1886 - 1890
• a: 11.4401 ± 0.0002 Å
• b: 16.7063 ± 0.0003 Å
• c: 16.3663 ± 0.0003 Å
• α: 90°
• β: 90.6112 ± 0.0016°
• γ: 90°
• Cell volume: 3127.78 ± 0.1 ų
• Cell temperature: 150.01 ± 0.1 K
• Ambient diffraction temperature: 150.01 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.056
• Residual factor for significantly intense reflections: 0.0355
• Weighted residual factors for significantly intense reflections: 0.0629
• Weighted residual factors for all reflections included in the refinement: 0.0708
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No