Information card for entry 7037604

Structure parameters

• Formula: C147.5 H173.5 Mn N4
• Calculated formula: C147.5 H173.5 Mn N4
• Title of publication: Stabilisation of carbonyl free amidinato-manganese(ii) hydride complexes: "masked" sources of manganese(i) in organometallic synthesis.
• Authors of publication: Fohlmeister, Lea; Jones, Cameron
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 4
• Pages of publication: 1436 - 1442
• a: 17.7667 ± 0.0004 Å
• b: 19.5336 ± 0.0005 Å
• c: 20.8577 ± 0.0005 Å
• α: 72.13 ± 0.002°
• β: 67.919 ± 0.002°
• γ: 78.661 ± 0.002°
• Cell volume: 6356.9 ± 0.3 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0842
• Residual factor for significantly intense reflections: 0.0613
• Weighted residual factors for significantly intense reflections: 0.1776
• Weighted residual factors for all reflections included in the refinement: 0.2003
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No