Information card for entry 7037955

Structure parameters

• Formula: C54 H24 Cu10 N18 O4
• Calculated formula: C54 H24 Cu10 N18 O4
• Title of publication: An unprecedented 2D copper(i)-cyanide complex with 20-membered metal rings: the effect of the co-ligand 4,5-diazafluoren-9-one.
• Authors of publication: Ma, Feng; Gao, Su-Mei; Wu, Meng-Meng; Zhao, Jiong-Peng; Liu, Fu-Chen; Li, Nai-Xuan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 7
• Pages of publication: 2796 - 2799
• a: 8.0131 ± 0.0016 Å
• b: 11.455 ± 0.002 Å
• c: 15.705 ± 0.003 Å
• α: 86.68 ± 0.03°
• β: 84.63 ± 0.03°
• γ: 73.35 ± 0.03°
• Cell volume: 1374.3 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0833
• Residual factor for significantly intense reflections: 0.0504
• Weighted residual factors for significantly intense reflections: 0.0817
• Weighted residual factors for all reflections included in the refinement: 0.0893
• Goodness-of-fit parameter for all reflections included in the refinement: 1.108
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No