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Information card for entry 7037956
Preview
Coordinates | 7037956.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H42 N2 P2 Si4 |
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Calculated formula | C24 H42 N2 P2 Si4 |
Title of publication | Cyclometalated titanium and zirconium complexes stabilised by a new silylmethylene-linked tetradentate triamidophosphine. |
Authors of publication | Sietzen, M.; Federmann, P.; Sonnenschein, C.; Wadepohl, H.; Ballmann, J. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2016 |
Journal volume | 45 |
Journal issue | 7 |
Pages of publication | 3013 - 3023 |
a | 7.1947 ± 0.0002 Å |
b | 8.3354 ± 0.0002 Å |
c | 13.4789 ± 0.0003 Å |
α | 86.273 ± 0.002° |
β | 78.908 ± 0.002° |
γ | 73.161 ± 0.003° |
Cell volume | 759.19 ± 0.04 Å3 |
Cell temperature | 110 ± 1 K |
Ambient diffraction temperature | 110 ± 1 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0488 |
Residual factor for significantly intense reflections | 0.0446 |
Weighted residual factors for significantly intense reflections | 0.1089 |
Weighted residual factors for all reflections included in the refinement | 0.1112 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.045 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.5418 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7037956.html
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