Information card for entry 7038000

Structure parameters

• Formula: C54 H111 Ge9 K O3 Si12
• Calculated formula: C54 H111 Ge9 K O3 Si12
• Title of publication: {Ge9[Si(SiMe3)3]2}(2-): a starting point for mixed substituted metalloid germanium clusters.
• Authors of publication: Kysliak, O.; Schnepf, A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 6
• Pages of publication: 2404 - 2408
• a: 12.1599 ± 0.0011 Å
• b: 15.058 ± 0.0014 Å
• c: 27.802 ± 0.003 Å
• α: 97.312 ± 0.002°
• β: 94.153 ± 0.002°
• γ: 108.939 ± 0.002°
• Cell volume: 4740.7 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0859
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for significantly intense reflections: 0.0937
• Weighted residual factors for all reflections included in the refinement: 0.1031
• Goodness-of-fit parameter for all reflections included in the refinement: 0.934
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No