Information card for entry 7038001

Structure parameters

• Formula: C44 H117 Ge9 K O3 Si12
• Calculated formula: C44 H112 Ge9 K O3 Si12
• Title of publication: {Ge9[Si(SiMe3)3]2}(2-): a starting point for mixed substituted metalloid germanium clusters.
• Authors of publication: Kysliak, O.; Schnepf, A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 6
• Pages of publication: 2404 - 2408
• a: 26.448 ± 0.004 Å
• b: 11.2469 ± 0.0018 Å
• c: 30.221 ± 0.004 Å
• α: 90°
• β: 112.221 ± 0.004°
• γ: 90°
• Cell volume: 8322 ± 2 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1146
• Residual factor for significantly intense reflections: 0.0562
• Weighted residual factors for significantly intense reflections: 0.1147
• Weighted residual factors for all reflections included in the refinement: 0.1339
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No