Information card for entry 7038234

Structure parameters

• Formula: C38 H34 Cl2 N8 O4 Pb2
• Calculated formula: C38 H34 Cl2 N8 O4 Pb2
• Title of publication: Concurrent agostic and tetrel bonding interactions in lead(ii) complexes with an isonicotinohydrazide based ligand and several anions.
• Authors of publication: Mahmoudi, Ghodrat; Bauzá, Antonio; Frontera, Antonio
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 12
• Pages of publication: 4965 - 4969
• a: 10.638 ± 0.0011 Å
• b: 19.076 ± 0.002 Å
• c: 9.2825 ± 0.001 Å
• α: 90°
• β: 103.396 ± 0.002°
• γ: 90°
• Cell volume: 1832.5 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0281
• Residual factor for significantly intense reflections: 0.0227
• Weighted residual factors for significantly intense reflections: 0.0497
• Weighted residual factors for all reflections included in the refinement: 0.0514
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No