Information card for entry 7038235

Structure parameters

• Formula: C19 H17 I N4 O2 Pb
• Calculated formula: C19 H13 I N4 O2 Pb
• SMILES: I[Pb]12[n]3c(cccc3)C(=[N]2N=C(O1)c1ccncc1)c1ccccc1.OC
• Title of publication: Concurrent agostic and tetrel bonding interactions in lead(ii) complexes with an isonicotinohydrazide based ligand and several anions.
• Authors of publication: Mahmoudi, Ghodrat; Bauzá, Antonio; Frontera, Antonio
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 12
• Pages of publication: 4965 - 4969
• a: 10.9695 ± 0.0009 Å
• b: 19.2524 ± 0.001 Å
• c: 9.5858 ± 0.0008 Å
• α: 90°
• β: 105.181 ± 0.009°
• γ: 90°
• Cell volume: 1953.8 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0829
• Residual factor for significantly intense reflections: 0.0585
• Weighted residual factors for significantly intense reflections: 0.1503
• Weighted residual factors for all reflections included in the refinement: 0.1601
• Goodness-of-fit parameter for all reflections included in the refinement: 1.003
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No