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Information card for entry 7038369
Preview
Coordinates | 7038369.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30 H60 F10 O4 P4 Rh2 |
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Calculated formula | C30 H60 F10 O4 P4 Rh2 |
SMILES | C([P](CC)([Rh]12(O[O]1[Rh]1([O]2O1)([P](CC)(CC)CC)([P](CC)(CC)CC)C(=C(\F)C(F)(F)F)\F)(/C(=C(F)\C(F)(F)F)F)[P](CC)(CC)CC)CC)C |
Title of publication | Synthesis of a rhodium(i) germyl complex: a useful tool for C-H and C-F bond activation reactions. |
Authors of publication | Ahrens, Theresia; Ahrens, Mike; Braun, Thomas; Braun, Beatrice; Herrmann, Roy |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2016 |
Journal volume | 45 |
Journal issue | 11 |
Pages of publication | 4716 - 4728 |
a | 10.3168 ± 0.0005 Å |
b | 18.2065 ± 0.0009 Å |
c | 11.2497 ± 0.0006 Å |
α | 90° |
β | 95.38 ± 0.002° |
γ | 90° |
Cell volume | 2103.75 ± 0.18 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0334 |
Residual factor for significantly intense reflections | 0.0232 |
Weighted residual factors for significantly intense reflections | 0.0517 |
Weighted residual factors for all reflections included in the refinement | 0.0549 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.063 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7038369.html
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Users of the data should acknowledge the original authors of the
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