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Information card for entry 7038368
Preview
Coordinates | 7038368.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30 H60 F10 O4 P4 Rh2 |
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Calculated formula | C30 H60 F10 O4 P4 Rh2 |
SMILES | C(C)[P](CC)(CC)[Rh]12([O](O1)[Rh]1([O]2O1)([P](CC)(CC)CC)([P](CC)(CC)CC)/C(=C(F)\C(F)(F)F)F)([P](CC)(CC)CC)C(=C(\F)C(F)(F)F)\F |
Title of publication | Synthesis of a rhodium(i) germyl complex: a useful tool for C-H and C-F bond activation reactions. |
Authors of publication | Ahrens, Theresia; Ahrens, Mike; Braun, Thomas; Braun, Beatrice; Herrmann, Roy |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2016 |
Journal volume | 45 |
Journal issue | 11 |
Pages of publication | 4716 - 4728 |
a | 11.5052 ± 0.0014 Å |
b | 11.7794 ± 0.0012 Å |
c | 15.3559 ± 0.0017 Å |
α | 90° |
β | 92.7 ± 0.005° |
γ | 90° |
Cell volume | 2078.8 ± 0.4 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0235 |
Residual factor for significantly intense reflections | 0.0211 |
Weighted residual factors for significantly intense reflections | 0.0571 |
Weighted residual factors for all reflections included in the refinement | 0.0588 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.008 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7038368.html
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Users of the data should acknowledge the original authors of the
structural data.